Spectris SERVOPRO Chroma User manual

Part Number: 04400001A

Revision: 7

Language: UK English

SERVOPRO Chroma

OPERATOR MANUAL

SERVOPRO CHROMA Gas Analyser

1 04400001A / Revision 7

SERVOPRO CHROMA Gas Analyser

2 04400001A / Revision 7

TABLE OF CONTENT

Section Page

1Description and Definitions ........................................................................................ 9

1.1 Scope of this manual........................................................................................... 9

1.2 Safety information .............................................................................................. 9

1.3 Description of Chroma Gas Analyser ............................................................... 10

1.3.1 Introduction................................................................................................. 10

1.3.2 Plasma Emission Detector (PED) ............................................................... 11

1.3.3 Flame Ionisation Detector (FID)................................................................. 11

1.3.4 Thermal Conductivity Detector (TCD)....................................................... 12

1.3.5 Signal conditioning ..................................................................................... 12

1.3.6 Main PC and graphic display...................................................................... 12

1.3.7 Oven heater and control .............................................................................. 12

1.3.8 I/O board ..................................................................................................... 13

1.4 Description of Analyser Rear Connections....................................................... 14

1.4.1 SERVOPRO Chroma Complete Rear Connections.................................... 14

1.4.2 SERVOPRO Chroma Reduced Rear Connections ..................................... 15

1.5 Auxiliary Oven.................................................................................................. 17

1.5.1 Description of Auxiliary Oven.................................................................... 17

1.5.2 Auxiliary Oven Rear Connections .............................................................. 17

1.6 Standalone PC Rear Connections ..................................................................... 18

2Software license ........................................................................................................ 20

2.1 MICROSOFT SOFTWARE LICENSE TERM ............................................... 20

3Specifications............................................................................................................ 31

3.1 General.............................................................................................................. 32

3.2 Gas .................................................................................................................... 33

3.3 Ovens Specification .......................................................................................... 34

3.4 Environmental Limits ....................................................................................... 34

3.5 Digital Relay Outputs ....................................................................................... 34

3.6 4-20 mA Outputs............................................................................................... 35

3.7 Digital Inputs .................................................................................................... 35

3.8 Hydrogen Relay Output .................................................................................... 36

3.9 Ethernet Port ..................................................................................................... 36

3.10 RS-232 Port....................................................................................................... 36

3.11 RS-485 Port....................................................................................................... 37

3.12 USB Connector ................................................................................................. 37

3.13 Mains input cables (Master/Secondary/Standalone PC)................................... 37

4THE USER INTERFACE......................................................................................... 38

4.1 User Interface Controls ..................................................................................... 38

4.1.1 Edit Box control.......................................................................................... 38

4.1.2 Radio control............................................................................................... 38

4.1.3 Slide control ................................................................................................ 39

4.1.4 Push button control ..................................................................................... 39

4.1.5 Grid control................................................................................................. 40

SERVOPRO CHROMA Gas Analyser

3 04400001A / Revision 7

4.1.6 Combo control ............................................................................................ 40

4.1.7 Check Box control ...................................................................................... 41

4.1.8 Tab control .................................................................................................. 41

4.2 User Interface Menu Description...................................................................... 42

4.3 Run Menu.......................................................................................................... 42

4.3.1 Real Time Chromatogram Menu ................................................................ 42

4.3.2 Start Button (F2) ......................................................................................... 43

4.3.3 Injection Mode ............................................................................................ 44

4.3.4 Injection Status............................................................................................ 44

4.3.5 Historic Values (F3).................................................................................... 44

4.3.6 Historic Alarm (F4)..................................................................................... 44

4.3.7 Range (F5) .................................................................................................. 44

4.3.8 Save (F6)..................................................................................................... 45

4.3.9 Undo Zoom (F8) ......................................................................................... 45

4.3.10 Print (Alt F2)............................................................................................... 46

4.3.11 Remote Countdown .................................................................................... 46

4.4 Historic Menu ................................................................................................... 46

4.4.1 Alarm Menu ................................................................................................ 46

4.5 Diagnostic Menu............................................................................................... 49

4.5.1 Diagnostic ................................................................................................... 49

4.5.2 Analyse Chromatogram .............................................................................. 52

4.5.3 Trending...................................................................................................... 55

4.5.4 Advanced Diagnostic .................................................................................. 58

4.6 Configuration Menu.......................................................................................... 60

4.6.1 System......................................................................................................... 60

4.6.2 Proportional Integral Derivative (PID) ....................................................... 64

4.6.3 Flow ............................................................................................................ 65

4.6.4 Cycle ........................................................................................................... 66

4.6.5 Date & Time ............................................................................................... 73

4.6.6 Advanced Configuration............................................................................. 74

4.6.7 Alarm .......................................................................................................... 80

4.6.8 Printers ........................................................................................................ 81

4.6.9 Export the Analyser Configuration............................................................. 82

4.7 Analyser Calibration ......................................................................................... 83

4.7.1 Noise Threshold (THRSH) Calibration ...................................................... 83

4.7.2 Span calibration .......................................................................................... 84

4.8 Calibration of the 4-20mA outputs ................................................................... 87

4.9 Remote .............................................................................................................. 88

4.9.1 Report Software .......................................................................................... 88

4.9.2 Remote Control........................................................................................... 89

4.10 About................................................................................................................. 90

4.10.1 Chromatogram saving................................................................................. 91

4.10.2 Quit ............................................................................................................. 92

5UNPACK THE ANALYSER ................................................................................... 93

6Installation and Setup................................................................................................ 94

6.1 Electrical installation ........................................................................................ 94

SERVOPRO CHROMA Gas Analyser

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6.1.1 Electrical safety........................................................................................... 94

6.1.2 Master chassis electrical connections ......................................................... 95

6.1.3 Master chassis with Secondary chassis electrical connections ................... 97

6.1.4 Stand-alone PC with Secondary chassis electrical connections ................. 99

6.2 Master/Secondary Chassis rear panel electrical connections.......................... 102

6.2.1 Digital input .............................................................................................. 102

6.2.2 Digital output contacts .............................................................................. 102

6.2.3 4-20 mA outputs ....................................................................................... 103

6.2.4 RS-485 port............................................................................................... 105

6.2.5 RS-232 port............................................................................................... 105

6.2.6 Auxiliary oven port ................................................................................... 105

6.2.7 FID fuel shut-off relay/Hydrogen relay output......................................... 106

6.3 Gas installation................................................................................................ 107

6.3.1 Choosing the right materials for the sampling system.............................. 107

6.3.2 Carrier Gas Hardware Selection ............................................................... 108

6.3.3 Gas Connections - Rear Panel................................................................... 109

1. Master and Secondary Chassis.................................................................. 109

2. Auxiliary Oven.......................................................................................... 110

7START-UP AND SHUTDOWN PROCEDURE ................................................... 111

7.1 Equipment/Tools............................................................................................. 111

7.2 Installation requirements................................................................................. 111

7.3 Start-up procedure........................................................................................... 111

7.4 Shut-down procedure ...................................................................................... 113

8ROUTINE MAINTENANCE................................................................................. 114

9STORAGE AND DISPOSAL ................................................................................ 115

9.1 Storage ............................................................................................................ 115

9.2 Disposal........................................................................................................... 115

10 COMPLIANCE....................................................................................................... 116

11 RS-232 ADDENDUM ............................................................................................ 117

11.1 Start analysis ................................................................................................... 117

11.2 Analyser status ................................................................................................ 117

11.3 Send results ..................................................................................................... 118

11.4 Enable-Disable Calibration............................................................................. 119

11.5 Respan............................................................................................................. 119

11.6 Change Configuration..................................................................................... 119

12 FID ADDENDUM.................................................................................................. 120

12.1 FID Advanced Configuration –General Menu .............................................. 120

12.2 FID Advanced Configuration - FID Menu ..................................................... 121

12.3 FID Advanced Configuration –Detector Menu ............................................. 123

12.4 FID Advanced Configuration –Flow Menu................................................... 124

12.5 FID Advanced Configuration –Oven Menu .................................................. 125

12.6 FID Monitoring and Configuration Menus..................................................... 126

12.7 FID Diagnostic-Diagnostic Menu................................................................... 129

12.8 FID Cycle Configuration Menu ...................................................................... 130

12.9 FID Startup...................................................................................................... 131

12.10 FID System Errors .......................................................................................... 132

SERVOPRO CHROMA Gas Analyser

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12.11 FID Troubleshooting....................................................................................... 134

13 ANALYSER TROUBLE SHOOTING .................................................................. 135

14 PRODUCT DISPOSAL –WEEE Directive........................................................... 139

15 REACH REGULATION ........................................................................................ 139

SERVOPRO CHROMA Gas Analyser

6 04400001A / Revision 7

LIST OF TABLES

Table name Page

Table 1 : I/O board............................................................................................................ 13

Table 2 : General Specification......................................................................................... 32

Table 3 : Gas Specification ............................................................................................... 33

Table 4 : Ovens specification............................................................................................ 34

Table 5 : Environmental limits ......................................................................................... 34

Table 6 : Digital relay outputs .......................................................................................... 34

Table 7 : 4-20 mA outputs ................................................................................................ 35

Table 8 : Digital inputs ..................................................................................................... 35

Table 9 : Hydrogen relay output ....................................................................................... 36

Table 10 : Ethernet cable .................................................................................................. 36

Table 11 : RS-232 port..................................................................................................... 36

Table 12 : RS-485 port...................................................................................................... 37

Table 13 : USB port .......................................................................................................... 37

Table 14 : Mains cable...................................................................................................... 37

Table 15 : Diagnostic menu .............................................................................................. 51

Table 16 : Diagnostic menu –manual checks .................................................................. 51

Table 17 : Diagnostic-Analyse Chromatogram menu ...................................................... 54

Table 18 : Trending menu –summary of functions.......................................................... 57

Table 19 : Oven set point .................................................................................................. 62

Table 20 : Peak Configuration Columns........................................................................... 68

Table 21 : Peak Data......................................................................................................... 68

Table 22 : Peak Configuration Menu................................................................................ 68

Table 23 : Digital Output Contacts ................................................................................. 102

Table 24 : 4-20 mA connections and associated fuses ................................................... 104

Table 25 : RS-232 Start Analysis.................................................................................... 117

Table 26 : RS-232 Analyser Status................................................................................. 117

Table 27 : RS-232 Send Results ..................................................................................... 118

Table 28 : RS-232 Enable-Disable Calibration .............................................................. 119

Table 29 : RS-232 Respan .............................................................................................. 119

Table 30 : RS-232 Change Configuration ...................................................................... 119

Table 31 : Advanced FID menu parameters ................................................................... 121

Table 32 : Gas flow set point .......................................................................................... 131

Table 33 : Gas flow set point 2 ....................................................................................... 131

Table 34 : Gas ignition Point .......................................................................................... 131

Table 35 : FID Troubleshooting ..................................................................................... 134

Table 36 : Troubleshooting Typical Issues –Symptoms................................................ 135

Table 37 : Troubleshooting Typical Issues –Likely Causes .......................................... 136

Table 38 : Troubleshooting Typical Issues –Potential Solutions .................................. 138

SERVOPRO CHROMA Gas Analyser

7 04400001A / Revision 7

LIST OF FIGURES

Figure name Page

Figure 1 : SERVOPRO Chroma complete rear connections ............................................ 14

Figure 2 : SERVOPRO Chroma reduced rear connections .............................................. 15

Figure 3 : Gas connections when FID Detector fitted ...................................................... 16

Figure 4 : Auxiliary Oven rear connections...................................................................... 17

Figure 5 : Standalone PC rear connections ....................................................................... 18

Figure 6: Edit Box control ................................................................................................ 38

Figure 7 : Radio control .................................................................................................... 38

Figure 8 : Slide control ..................................................................................................... 39

Figure 9 : Button control................................................................................................... 39

Figure 10 : Grid control .................................................................................................... 40

Figure 11 : Combo Box control ........................................................................................ 40

Figure 12 : Check Box control.......................................................................................... 41

Figure 13 : Tab Box control.............................................................................................. 41

Figure 14 : Menu Structure ............................................................................................... 42

Figure 15 : Run - Real time menu..................................................................................... 43

Figure 16 : Peak Grid –Alarm Status display colours...................................................... 45

Figure 17 : Diagnostic menu............................................................................................. 49

Figure 18 : Diagnostic –Analyse Chromatogram ............................................................ 52

Figure 19 : Diagnostic - Trending menu........................................................................... 55

Figure 20 : Trending menu valve state ............................................................................. 57

Figure 21 : Diagnostic - Advanced Diagnostic menu....................................................... 58

Figure 22 : Configuration - System menu......................................................................... 60

Figure 23 : Configuration-PID menu................................................................................ 64

Figure 24 : Configuration-Flow menu .............................................................................. 65

Figure 25 : Configuration-Cycle menu ............................................................................. 66

Figure 26 : Cycle-Peak Configuration menu .................................................................... 67

Figure 27 : Peak detection configuration menu ................................................................ 69

Figure 28 : Valve configuration menu .............................................................................. 70

Figure 29 : Typical sequence for valve timing ................................................................. 70

Figure 30 : Flow timing configuration menu.................................................................... 71

Figure 31 : Date and Time menu ...................................................................................... 73

Figure 32 : Advanced configuration-General menu ......................................................... 74

Figure 33 : Advanced configuration-Detector menu ........................................................ 76

Figure 34 : Advanced configuration-Flow menu.............................................................. 77

Figure 35 : Advanced configuration-Valve menu ............................................................ 78

Figure 36 : Advanced configuration-Oven menu ............................................................. 79

Figure 37 : Configuration Alarm menu ............................................................................ 80

Figure 38 : Printers configuration menu ........................................................................... 81

Figure 39 : Calibration menu ............................................................................................ 83

Figure 40 : Calibration-Span menu................................................................................... 85

Figure 41 : Calibration- 4-20 mA outputs calibration menu............................................. 87

SERVOPRO CHROMA Gas Analyser

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Figure 42 : Remote-Remote software menu ..................................................................... 88

Figure 43 : Remote-Remote control menu........................................................................ 89

Figure 44 : About menu .................................................................................................... 90

Figure 45 : Historic-Chromatogram saving menu ............................................................ 91

Figure 46 : Master chassis electrical connections............................................................. 95

Figure 47 : Master with secondary chassis, electrical connections .................................. 97

Figure 48 : Master with 2 Secondary Chassis, electrical connections.............................. 98

Figure 49 : Stand-alone PC with secondary, electrical connections............................... 100

Figure 50 : Stand-alone PC with two Secondarys, electrical connections...................... 101

Figure 51 : Digital input connection ............................................................................... 102

Figure 52 : Digital outputs connection............................................................................ 103

Figure 53 : 4-20 mA schematic and external connections.............................................. 104

Figure 54 –Connecting a fuel shut-off valve ................................................................. 106

Figure 55: Advanced menu............................................................................................. 120

Figure 56: Advanced Configuration FID menu .............................................................. 121

Figure 57: Advanced Detector menu .............................................................................. 123

Figure 58: Advanced Configuration Flow menu ............................................................ 124

Figure 59: Advanced oven menu .................................................................................... 125

Figure 60: Monitoring System Configuration menu....................................................... 126

Figure 61: Monitoring Real Time Chromatogram menu................................................ 126

Figure 62: Monitoring Trending menu ........................................................................... 127

Figure 63: Monitoring PID Configuration menu............................................................ 127

Figure 64: Monitoring Flow Configuration menu .......................................................... 128

Figure 65 : Diagnostic menu........................................................................................... 129

Figure 66: Cycle Configuration menu ............................................................................ 130

Figure 67 :The WEEE label............................................................................................ 139

SERVOPRO CHROMA Gas Analyser

9 04400001A / Revision 7

1 DESCRIPTION AND DEFINITIONS

1.1 Scope of this manual

This manual provides installation, operation and routine maintenance instructions

for the SERVOPRO Chroma Online Trace Gas analyser, abbreviated to

“SERVOPRO Chroma”or “analysers” where applicable in the reminder of this

manual.

1.2 Safety information

Read this manual and ensure that you fully understand its content before you

attempt to install, use or maintain the SERVOPRO Chroma. Important safety

information is highlighted in this manual as WARNINGs and CAUTIONs, which

are used as follows.

WARNING

Warnings highlight specific hazards which, if not addressed, may

result in personal injury or death.

CAUTION

Cautions highlight hazards which, if not addressed, can result in damage

to the SERVOPRO Chroma or other equipment or property.

This manual also incorporates “Be aware of” information, which is used as follows:

This highlights information which it is useful for you to be aware

of (for example, specific operating conditions, and so on).

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