Restek ProFLOW 6000 Series User manual

www.restek.com

Restek ProFLOW 6000

Electronic Flowmeter

Version 5.6

(Cat.# 22656)

Instruction

Manual

2 www.restek.com

Table of Contents

1.0 Introduction ............................................................................................................................................. 3

2.0 Specifications........................................................................................................................................... 4

3.0 Installing the batteries ......................................................................................................................... 4

4.0 Battery power consumption.............................................................................................................. 5

4.1 Battery lifetime.............................................................................................................................. 5

4.2 Battery charge indicator ............................................................................................................ 5

5.0 Operating instructions ......................................................................................................................... 5

6.0 Interpreting results................................................................................................................................ 6

6.1 Flow range display....................................................................................................................... 6

7.0 Data collection on the PC ................................................................................................................... 7

8.0 ProFLOW 6000 menu structure......................................................................................................... 9

8.1 Unit power up/power down..................................................................................................... 9

8.2 USB activation................................................................................................................................ 9

8.3 Adjust LCD image backlight...................................................................................................10

8.4 Show battery charge indicator..............................................................................................10

8.5 Firmware version information ...............................................................................................11

8.6 Adjust auto shutoff duration..................................................................................................11

8.7 Display calibration date ...........................................................................................................12

8.8 Display unit serial number......................................................................................................12

9.0 Troubleshooting ...................................................................................................................................12

10.0 Product back label legend................................................................................................................13

11.0 Volumetric vs. mass flow measurements....................................................................................14

12.0 Bubble flowmeters ..............................................................................................................................14

13.0 Product case specifications..............................................................................................................14

14.0 Calibration and service ......................................................................................................................14

Declaration of Conformity ................................................................................................................31

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Restek ProFLOW 6000

Electronic Flowmeter

1.0 Introduction

Restek’s ProFLOW 6000 Flowmeter is specifically designed for use with gas chromatography (GC) systems. The

probe is applied directly to the gas flow stream, and the measured flow rate is presented on the LCD screen.

Units of flow are measured in mL/min.

This unit provides continuous real-time measurements of gas streams ranging from 0.50 mL/min to 500 mL/min.

Because the technology uses volumetric flow measurement, the unit is compatible with all laboratory gases.

CAUTION: Do NOT exceed maximum operating flow rates. Recalibration may be required if the unit

has been subjected to extreme flow rates.

Always use appropriate laboratory safety practices when operating this device. Wear laboratory

safety goggles when operating this unit.

NOTE: There are no serviceable parts in this unit. Opening the device—other than to change the batteries—or

tampering with the internal parts will void the factory warranty.

NOTE: To ensure accurate measurements and effective clearance of the flow gas from the unit, DO NOT

obstruct the vent holes on the back of the unit.

NOTE: Modifying the length of tubing can cause a shift in calibration.

Figure 1: Product diagrams

BACK

FRONT

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2.0 Specifications

Table I:

3.0 Installing the batteries

This unit uses two AA alkaline batteries.

To install batteries, extend the wire stand. Open the cover. Insert the batteries with the

polarity (⊕and ⊖) correctly aligned. Close the cover. (Figures 2 and 3.)

Precautions for battery replacement:

•Load the new batteries with their polarity (⊕ and ⊖) aligned correctly.

• Do not use rechargeable batteries.

Figure 2: Extend the wire stand before

opening battery door.

Figure 3

Insert the batteries

as marked.

–+

–

Type of measurement Volumetric flow

Accuracy of measurements ± 2% of flow reading or ± 0.2 mL/min, whichever is greater

Power requirements 2 AA alkaline batteries 1.5 V DC each/3 V DC 200 ma

Operating flow range 0.50 to 500 mL/min

Operating temperature range 32 °-120 °F (0 °- 48 °C)

Available communication USB type B data port

Warranty One year (excludes recalibration)

Calibration NIST traceable

Yearly recalibration is recommended

Certifications CE, Ex (see section 10.0)

Compliance WEEE, RoHS 2, China RoHS 2 (see section 10.0)

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NOTE: Store your ProFLOW 6000 in its protective storage case following use. Do not store this manual or any

other items on top of the ProFLOW 6000 or the unit may turn on when the storage case lid is closed.

4.0 Battery power consumption

4.1 Battery lifetime

The battery lifetime is dependent on the number of options the user has enabled.

The unit is shipped with the most energy-demanding options disabled (Table II).

The power saving functions can be changed.

èSee Section 8.2: USB Activation

èSee Section 8.3: Adjust LCD Image Backlight

èSee Section 8.6: Adjust Auto Shutoff Duration

Table II: Default settings for the ProFLOW 6000

Auto shutoff duration 6 minutes

LCD backlight 0 (off)

USB port disabled

4.2 Battery charge indicator

The unit includes a battery charge indicator. Replace batteries as needed.

èSee Section 8.4: Show Battery Charge Indicator

5.0 Operating instructions

CAUTION: Do not exceed maximum operating flow rates.

Recalibration may be required if the unit has been subjected to extreme flow rates.

Connect the white probe end tip to the output of the gas flow line to be measured. Be sure the probe tip

connection is completely sealed around the flow source outlet and is free of leaks (Figure 4). (White tubing ID

0.125"; OD 0.250")

Press and hold the (Power) button until the unit responds with a regular clicking sound. The Pro-

FLOW will immediately begin to provide flow measurements (Figure 5). Wait for the measured values to stabi-

lize. It takes a few seconds for the unit to reach a steady state with the gas flow line.

To power down the unit, press and hold the (Power) button until the unit stops clicking.

The unit is equipped with a timed auto shutoff option. (Default: 6 minutes.)

èSee Section 8.6: Adjust Auto Shutoff Duration

Figure 4: Probe connected to a GC gas outlet. Figure 5: LED displays the measured flow value.

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6.0 Interpreting results

The unit has an operating range of 0.50 mL/min to 500 mL/min (Figure

7). If the flow is less than 0.50 mL/min., the display will read“under range.”

If the flow exceeds 515 mL/min, the display will read“over range.” Exces-

sively high flow rates may damage this unit.

NOTE: units of mL/min are equivalent to ccm.

6.1 Flow range display

The unit automatically adjusts the resolution of the display depending

on the flow range being measured. Table III shows the resolution of the

flow ranges.

Figure 6: Example flow value.

Figure 7: Description of flow ranges.

Table III: Display resolution vs. flow range.

Flow Range

Display reads

“under range”

Display reads

flow values

Display reads

“over range”

0.50 mL/min 515 mL/min

Flow range Display resolution (mL/min)

0.50–9.99 0.01

10.0–99.9 0.1

100–500 1

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7.0 Data collection on the PC

WARNING: ONLY connect USB cable to USB port while unit is OFF.

The ProFLOW 6000 provides you with a data stream of real-time flow values via the USB port (Figure 1, p. 3). In

order to use this feature, you must first install the appropriate FTDI Virtual Com Port (VCP) Driver available at:

http://www.ftdichip.com/Drivers/VCP.htm

The VCP driver will cause the ProFLOW to appear as a standard RS-232 port. This will work on any operating

system for which there is an FTDI VCP driver. After installing the driver, connecting the device, and determining

which port it creates, you can access the data stream through any programmatic means, or by using any serial

terminal software.

For Windows systems:

To determine which port the ProFLOW is using, go to the Control Panel and open System. Go to the Hardware

tab and click the Device Manager button. Expand the Ports (COM & LPT) entry. Make sure the VCP driver is

installed and then connect a powered ProFLOW 6000 to the USB port. You will see the new COM port appear.

Open your serial terminal.

èSee Section 8.2: USB Activation

Figure 8: Screen capture of data collection.

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If you do not already have serial terminal software, free, open-source options are available online (i.e.,

RealTerm, etc.). You can download RealTerm* software from:

http://realterm.sourceforge.net/

After installation, click the Port tab and set the following:

Baud: 115200

Port: The appropriate VCP for your ProFLOW

Parity: None

Data Bits: 8 bits

Stop Bits: 1 bit

HardwareFlow Control: None

Go to the USB menu entry in the ProFLOW and turn the transmission on. Finally, click Open on the Port tab in

RealTerm and you will see the serial data stream begin in the terminal window (Figure 8).

If you would like to log the flow data, this can be done by clicking on the Capture tab. Set File to the name

and location of the log file that you would like to save and click either the Start: Overwrite or Start: Append

buttons appropriately (Figure 9).

*This software is not supplied or supported by Restek. User assumes all responsibility for the downloading and use of the program.

Figure 9: Screen capture of data collection.

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8.0 ProFLOW 6000 menu structure

8.1 Unit power up/power down

Press the (Power) button:

The LCD screen will display Followed by Followed by measured

the device intro screen: calibrated date: flow data:

01/10/2012

To power off, press and hold the (Power) button.

Other messages encountered at power up

If the unit is hooked up to a flow stream with a flow rate less than 0.50 mL/min,

the unit will report an“under range”status for the flow. This message will appear

until the flow rate exceeds 0.50 mL/min.

8.2 USB activation

To enable the USB, press the (Menu) button.

Use the (arrow) keys to select the USB menu:

Press the (menu) button again to enter the value select screen.

Use the (arrow) keys to toggle between USB “on”and“off.”

To return to the main menu screen, press the (menu) button.

To exit and return to measuring flow, press the (menu) button again.

èSee Section 7.0: Data Collection on the PC

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8.3 Adjust LCD image backlight

Press the (Menu) button.

Use the (arrow) keys to select the Backlight menu:

Press the (Menu) button again to enter the value select screen.

Use the (arrow) keys to select the backlight value.

Backlight Values: 0 (off) and 5 (maximum).

To return to the main menu screen, press the (Menu) button.

To exit and return to measuring flow, press the (Menu) button again.

8.4 Show battery charge indicator

Press the (Menu) button.

Use the (arrow) keys to select the Batteries menu:

Press the (Menu) button again.

The battery life is displayed.

To return to the main menu screen, press the (Menu) button.

To exit and return to measuring flow, press the (Menu) button again.

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