NIC-600-2266-03
Table of Contents
5
6.4 PREPARATION FOR MEASUREMENT ................................................................................ 69
6.4.1 Supply carrier gas................................................................................................ 69
6.4.2 Drain the gas-liquid separation bottle.................................................................. 69
6.4.3 Start up the PE1000Win application.................................................................... 70
6.4.4 Power up the PE-1............................................................................................... 70
6.4.5 Self-checks........................................................................................................... 70
6.4.6 Set the syringe wash solution.............................................................................. 71
6.5 SET MEASUREMENT CONDITIONS................................................................................... 72
6.5.1 Set measurement conditions ............................................................................... 72
6.5.2 Set table conditions.............................................................................................. 74
6.6 MEASUREMENTS........................................................................................................... 75
6.6.1 Perform a purge measurement............................................................................ 75
6.6.2 Set samples.......................................................................................................... 75
6.6.3 Select a measurement protocol........................................................................... 76
6.6.4 Set the number of injections................................................................................ 76
6.6.5 Select a measurement range............................................................................... 76
6.6.6 Register the mercury weight of the standard sample and unknown sample name............... 77
6.6.7 Start measurement............................................................................................... 78
6.6.8 Measurement end................................................................................................ 79
6.6.9 Aborting measurements....................................................................................... 79
6.6.10 Viewing measurement results............................................................................ 80
6.7 PRINTING REPORTS....................................................................................................... 81
6.8AFTER MEASUREMENT ENDS.......................................................................................... 81
7. MAINTENANCE............................................................................................................... 82
7.1 EQUIPMENT CHECKS ..................................................................................................... 82
7.1.1 Daily checks......................................................................................................... 82
7.1.2 Yearly checks ....................................................................................................... 84
7.2 ERRORS AND WARNINGS................................................................................................ 85
7.3 TROUBLESHOOTING ...................................................................................................... 87
7.3.1 If peak sensitivity decreases................................................................................ 87
7.3.2 Blank sample reading error.................................................................................. 88
7.3.3 Flowchart.............................................................................................................. 89
7.4 MAINTENANCE .............................................................................................................. 89
6.5.1.1 Mode.........................................................................................................72
6.5.1.2 Set up standard sample checks................................................................72
6.5.1.3 Set up blank sample checks.....................................................................73
