Table of Contents
1Contact information .............................................................................................................................. 5
2Notes on the Manual ............................................................................................................................. 5
2.1 Explanations of the Safety Instructions ............................................................................................. 6
2.2 General Safety Instructions ............................................................................................................... 8
2.3 Intended use...................................................................................................................................... 9
2.4 Improper use...................................................................................................................................... 9
2.5 Explanation of signs and symbols ..................................................................................................... 9
3Packaging, Transport and Installation .............................................................................................. 10
3.1 Packaging........................................................................................................................................ 10
3.2 Transport.......................................................................................................................................... 11
3.3 Conditions for the Installation Site................................................................................................... 11
3.4 Type Plate Description..................................................................................................................... 12
4Pre-installation guide.......................................................................................................................... 13
5Installation............................................................................................................................................ 16
5.1 Setting check up .............................................................................................................................. 16
5.2 Front Panel Illustration..................................................................................................................... 18
5.3 Installation of Furnace Covers for Manual and Loader Setups....................................................... 20
5.3.1 Manual Setup............................................................................................................................... 20
5.3.2 Autoloader Setup......................................................................................................................... 21
5.4 Mains power Connections ............................................................................................................... 21
5.5 Data Interface .................................................................................................................................. 23
5.6 Oxygen Connection ......................................................................................................................... 24
5.7 Operation Modes ............................................................................................................................. 26
5.8 Adjusting the gas flow...................................................................................................................... 27
5.9 Temperature adjustment.................................................................................................................. 28
5.10 Preheating the furnace .................................................................................................................... 28
5.10.1 Configuration of preheating ..................................................................................................... 28
5.10.2 BIOS-configuration .................................................................................................................. 29
6Analysis................................................................................................................................................ 30
6.1 Working procedure .......................................................................................................................... 30
6.1.1 Procedure of carrying out analyses with autoloader, optional..................................................... 32
6.1.2 Procedure of carrying out analyses with manual loading of the sample ..................................... 33
6.2 TIC-determination (optional)............................................................................................................ 34
6.2.1 TIC-module.................................................................................................................................. 34
6.2.2 TIC analysis................................................................................................................................. 34
6.2.3 TIC-module installation................................................................................................................ 36
6.2.4 TIC-module Operation procedure................................................................................................ 37
6.3 Applications...................................................................................................................................... 38
6.3.1 Coal.............................................................................................................................................. 38
6.3.2 Calcium Carbonate...................................................................................................................... 38
6.3.3 Graphite....................................................................................................................................... 38
6.3.4 Limestone .................................................................................................................................... 39
6.3.5 Oil, Asphalt and Rubber............................................................................................................... 39
6.3.6 Wood............................................................................................................................................ 39
7Maintenance......................................................................................................................................... 40
7.1 General information ......................................................................................................................... 40
7.2 Cleaning........................................................................................................................................... 41
7.3 Reagent tubes filling ........................................................................................................................ 42
7.3.1 Reagent tube replacing................................................................................................................ 42
7.3.2 Filling quantities........................................................................................................................... 44
7.4 Moisture trap replacing (furnace)..................................................................................................... 47
7.5 O-rings replacement........................................................................................................................ 48
