Metrohm 6.5330.210 User manual

IC equipment

IC equipment: Inline Ultrafiltration – MiPT (6.5330.210)

Manual

8.110.8039EN / 2019-10-25

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

IC equipment

IC equipment: Inline Ultrafiltration –

MiPT (6.5330.210)

Manual

8.110.8039EN / 2019-10-25

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

IC equipment: Inline Ultrafiltration – MiPT ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Description of the IC equipment: Inline Ultrafiltration –

MiPT ....................................................................................... 1

1.2 About the documentation ................................................... 2

1.2.1 Symbols and conventions ........................................................ 3

2 Overview 4

2.1 Parts of the IC equipment: Inline Ultrafiltration –

MiPT ....................................................................................... 4

2.2 Components of the ultrafiltration cell ................................ 5

2.3 Connectors of the ultrafiltration cell ................................... 6

2.4 Components of the Liquid Handling Station ...................... 7

3 Mode of operation of the intelligent Partial Loop Injection

Technique 8

4 Installation 10

4.1 Installing the ultrafiltration cell ......................................... 10

4.1.1 Preparing the ultrafiltration cell .............................................. 10

4.1.2 Connecting the ultrafiltration cell ........................................... 14

4.1.3 Inserting the ultrafiltration cell ............................................... 17

4.1.4 Deaerating the ultrafiltration cell ............................................ 17

4.2 Equipping the ultrapure water bottle ............................... 19

4.3 Installing the Dosino .......................................................... 20

4.3.1 Installing the Dosino .............................................................. 20

4.3.2 Connecting the dosing unit with the ultrapure water bottle ... 22

4.3.3 Connecting the dosing unit to the injection valve ................... 23

4.3.4 Connecting the dosing unit to the waste container ................ 24

4.4 Exchanging the sample loop ............................................. 26

4.5 Connecting the Liquid Handling Station .......................... 26

5 Operation and maintenance 29

5.1 Operation ............................................................................ 29

5.1.1 Service life of the filtration membrane .................................... 29

5.1.2 Selecting the filtration membrane .......................................... 30

5.2 Maintenance ....................................................................... 31

5.2.1 Replacing the filtration membrane ......................................... 31

5.2.2 Maintenance of the dosing unit (6.3032.120) ........................ 32

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ IC equipment: Inline Ultrafiltration – MiPT

6 Technical specifications 33

6.1 Ultrafiltration cell (6.2729.110) ......................................... 33

6.2 Filtration membrane (6.2714.020) .................................... 33

6.3 Liquid Handling Station (6.2841.120) ............................... 33

6.4 Dosing unit 2 mL (6.3032.120) ......................................... 33

7 Accessories 34

Index 35

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

IC equipment: Inline Ultrafiltration – MiPT ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 IC equipment: Inline Ultrafiltration – MiPT – Overview ....................... 2

Figure 2 IC equipment: Inline Ultrafiltration – MiPT – Parts .............................. 4

Figure 3 Couplings, adapters and screws of the IC equipment: Inline Ultrafiltra-

tion – MiPT ....................................................................................... 5

Figure 4 Ultrafiltration cell – Parts .................................................................... 5

Figure 5 Ultrafiltration cell – Connectors ......................................................... 6

Figure 6 Liquid Handling Station – Parts .......................................................... 7

Figure 7 Connecting the ultrafiltration cell – Overview ................................... 10

Figure 8 Connecting the ultrafiltration cell ..................................................... 14

Figure 9 Equipping the ultrapure water bottle ............................................... 19

Figure 10 Connecting the Dosino – Overview .................................................. 20

Figure 11 Mounting the Dosino ...................................................................... 21

Figure 12 Mounting the FEP tubing ................................................................. 23

Figure 13 Installing the transfer capillary ......................................................... 24

Figure 14 Connecting to the waste container .................................................. 25

Figure 15 Connecting the Liquid Handling Station – Overview ......................... 26

Figure 16 Connecting the Liquid Handling Station ........................................... 26

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

IC equipment: Inline Ultrafiltration – MiPT ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Description of the IC equipment: Inline Ultrafiltra-

tion – MiPT

The IC equipment: Inline Ultrafiltration – MiPT (6.5330.210) contains all

the required accessory parts for the Inline Ultrafiltration and for the

Metrohm intelligent Partial Loop Injection Technique (MiPT).

Combining the Inline Ultrafiltration and MiPT allows for the samples to be

filtered and subsequently be filled into the sample loop with an accurately

measured volume.

The main component of the Inline Ultrafiltration is the high-performance

ultrafiltration cell. This cell is suitable for the filtration of samples that pose

particular requirements with regard to filtration effectiveness and sample

throughput.

MiPT allows you to fill the 250 µL sample loop with a precisely measured

volume. In this process, an 800 Dosino with a 2 mL dosing unit performs

the precise dosing increments. MiPT enables calibration with only one

standard solution, as the injection volume can be selected freely. The same

applies to sample injection. This means, for example, that a small injection

volume can be selected for a highly concentrated sample.

The sample needle is rinsed with ultrapure water in the rinsing unit of the

Liquid Handling Station (6.2841.120) after each sample aspiration. The

Liquid Handling Station (6.2841.120) can be mounted on any Sample Pro-

cessor equipped with a Swing Head.

1.2 About the documentation ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ IC equipment: Inline Ultrafiltration – MiPT

Figure 1 IC equipment: Inline Ultrafiltration – MiPT – Overview

1.2 About the documentation

This manual describes the installation of the IC equipment: Inline Ultrafil-

tration – MiPT.

CAUTION

Please read through this documentation carefully before putting the

equipment into operation. The documentation contains information

and warnings which the user must follow in order to ensure safe opera-

tion of the equipment.

Additional documentation

Topic Document

Mounting the Liquid Handling Station on

the Sample Processor

8.108.8011 Manual for Liquid Handling

Station

Installing the Dosino 8.800.8002 Manual for 800 Dosino

Care and maintenance of the dosing unit 8.807.8002 Manual for 807 Dosing Unit

Table of contents

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