Thermo Scientific 1371 User manual

Thermo Scientific Barnstead Nanopure™

TOC - Analytical Ultrapure Water System

Series 1371 and 1379

Operating Manual and Parts List LT1371X1 Rev. 1

_________________________________________________________________________________

Part of Thermo Fisher Scientific

Thermo Scientific

MANUAL NUMBER LT1371X1 (7007147)

1 26925 3/10/11 Decreased water pressure rating in Specifications from 100 to 80 psi ccs

0 -- 7/22/10 Transfer to Marietta (was LT1371X1 3/8/10) ccs

REV ECR/ECN DATE DESCRIPTION By

Preface

Nanopure TOC - Analytical i

Models covered in this manual

Model Number Voltage

D11941 (7147) 90-240V

D12411 (7151) 100-240V

Thermo Scientificii Nanopure TOC - Analytical

Preface

Important Read this instruction manual. Failure to read, understand and follow the instructions in this manual

may result in damage to the unit, injury to operating personnel, and poor equipment performance. s

Caution All internal adjustments and maintenance must be performed by qualified service personnel. s

Material in this manual is for information purposes only. The contents and the product it describes are subject to

change without notice. Thermo Fisher Scientific makes no representations or warranties with respect to this

manual. In no event shall Thermo be held liable for any damages, direct or incidental, arising out of or related to

the use of this manual.

Thermo Scientific Nanopure TOC - Analytical iii

Preface

Important operating and/or maintenance instructions. Read the accompanying text carefully.

Potential electrical hazards. Only qualified persons should perform procedures associated with this

symbol.

Equipment being maintained or serviced must be turned off and locked off to prevent possible injury.

Hot surface(s) present which may cause burns to unprotected skin, or to materials which may be

damaged by elevated temperatures.

Marking of electrical and electronic equipment, which applies to electrical and electronic equipment

falling under the Directive 2002/96/EC (WEEE) and the equipment that has been put on the market

after 13 August 2005.

This product is required to comply with the European Union’s Waste Electrical & Electronic

Equipment (WEEE) Directive 2002/96/EC. It is marked with the WEEE symbol. Thermo Fisher

Scientific has contracted with one or more recycling/disposal companies in each EU Member State

European Country, and this product should be disposed of or recycled through them. Further

information on Thermo’s compliance with this directive, the recyclers in your country and

information on Thermo products will be available at www.thermofisher.com.

4Always use the proper protective equipment (clothing, gloves, goggles, etc.)

4Always dissipate extreme cold or heat and wear protective clothing.

4Always follow good hygiene practices.

4Each individual is responsible for his or her own safety.

Thermo Scientificiv Nanopure TOC - Analytical

Preface

Do You Need Information or Assistance on

Thermo Scientific Products?

If you do, please contact us 8:00 a.m. to 6:00 p.m. (Eastern Time) at:

1-740-373-4763 Direct

1-800-438-4851 Toll Free, U.S. and Canada

1-877-213-8051 FAX

http://www.thermoscientific.com Internet Worldwide Web Home Page

Service E-Mail Address

Thermo Fisher Scientific

401 Millcreek Road, Box 649

Marietta, OH 45750

Our staff can provide information on pricing and give you quotations. We can

take your order and provide delivery information on major equipment items or make

arrangements to have your local sales representative contact you. Our products are listed on the

Internet and we can be contacted through our Internet home page.

Our staff can supply technical information about proper setup, operation or

troubleshooting of your equipment. We can fill your needs for spare or replacement parts or

provide you with on-site service. We can also provide you with a quotation on our Extended

Warranty for your Thermo Scientific products.

Whatever Thermo Scientific products you need or use, we will be happy to discuss your

applications. If you are experiencing technical problems, working together, we will help you

locate the problem and, chances are, correct it yourself...over the telephone without a service

call.

When more extensive service is necessary, we will assist you with direct factory trained

technicians or a qualified service organization for on-the-spot repair. If your service need is

covered by the warranty, we will arrange for the unit to be repaired at our expense and to your

satisfaction.

Regardless of your needs, our professional telephone technicians are available to assist you

Monday through Friday from 8:00 a.m. to 6:00 p.m. Eastern Time. Please contact us by

telephone or fax. If you wish to write, our mailing address is:

International customers, please contact your local Thermo Scientific distributor.

Sales Support

Service Support

service.led.marietta@thermofisher.com

Nanopure TOC - Analytical vThermo Scientific

Table of Contents

Safety Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-1

Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-1

General Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-1

Unpacking . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-1

Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-1

Choosing a Site . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-1

Wall Mounting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-2

Bench Mounting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-2

Other Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-2

Install Control Panel in a Remote Location . . . . . . . . . . . . . . . . . . . .5-3

Atmospheric Drain Connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-5

Feed Water Connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-5

Tubing Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-6

Electrical Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-7

Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6-1

Control Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6-1

Main Power Switch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6-1

Switches . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6-2

Initial Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7-1

Initial Rinse . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7-2

Cartridge Pack Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7-2

System Cleaning Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7-3

Normal Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8-1

Automatic Dispensing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8-2

Dispensing Water . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8-2

Section 1

Section 2

Section 3

Section 4

Section 5

Section 6

Section 7

Section 8

vi Nanopure TOC - Analytical Thermo Scientific

User Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-1

Setting the Displayed Language . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-1

Adjusting Display Brightness . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-1

Setting the Date and Time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-2

Setting the Cell Constant . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-3

Selecting the Setpoint . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-4

Use of Standby Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-4

Resetting the TOC Lamp Timer . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-5

Resetting the Cleaning Timer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-5

Using the TOC Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-6

Setting Volumetric Dispensing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-6

Change Purity Units: factory set - “MΩ-cm” . . . . . . . . . . . . . . . . . .9-7

Performing a System Flush . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-7

Setting Timed Dispensing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-7

Temperature Compensation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-8

Auto Standby . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-8

Unit Under Counter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9-9

Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10-1

Feed Water Float or Pressure Switch . . . . . . . . . . . . . . . . . . . . . . . . .10-1

Dispense Overflow Cutoff Float . . . . . . . . . . . . . . . . . . . . . . . . . . . .10-2

Electronic Calibration w/ N.I.S.T. Cal Module . . . . . . . . . . . . . . . .10-3

Manual/Accudispense Remote Dispensers . . . . . . . . . . . . . . . . . . . .10-4

Computer/Printer Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11-1

RS-232 Capture Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11-1

Procomm . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11-2

Connecting and Starting the Printer . . . . . . . . . . . . . . . . . . . . . . . .11-3

Printer Power Switch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11-3

Maintenance and Servicing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-1

Cell Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-1

System Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-2

System Depressurization . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-3

Cartridge Pack Replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-4

0.2 Micron Filter Replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-5

TOC Lamp Replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-6

Shutdown . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-7

Fuse Replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-7

Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13-1

Replacement Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14-1

Recommended Spares . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14-1

Ordering Procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14-3

Flow Chart . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14-4

Wiring Diagram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14-5

Table of Contents

Section 11

Section 12

Section 13

Section 14

Section 9

Section 10

Nanopure TOC - Analytical 1-1Thermo Scientific

Section 1 Safety Information

Your Thermo Scientific Barnstead Nanopure TOC - Analytical ultrapure

water system has been designed with function, reliability, and safety in

mind. It is your responsibility to install it in conformance with local

electrical codes. This manual contains important operating and safety

information. You must carefully read and understand the contents of this

manual prior to the use of this equipment. For safe operation, pay

attention to Notes, Cautions, and Warnings throughout the manual.

Water purification technology employs one or more of the following:

chemicals, electrical devices, mercury vapor lamps, steam and heated

vessels. Care should be taken when installing, operating or servicing

Barnstead products. The specific safety notes pertinent to this product are

listed below.

Warnings

To avoid electrical shock, always:

1. Use a properly grounded electrical outlet of correct voltage and current

handling capacity.

2. Do not locate the Nanopure TOC - Analytical directly over equipment

that requires electrical service. Routine maintenance of this unit may

involve water spillage and subsequent electrical shock hazard if

improperly located.

3. Replace fuses with those of the same type and rating.

4. Disconnect from the power supply prior to maintenance and servicing.

1-2 Nanopure TOC - Analytical Thermo Scientific

Section 1

Safety Information

To avoid personal injury:

1. Do not use in the presence of flammable or combustible materials;

fire or explosion may result. This device contains components which

may ignite such materials.

2. Use this device with water feed only. Sanitizing/cleaning agents must

be used in compliance with the instructions in this manual. Failure to

comply could result in explosion and personal injury.

3. Avoid splashing cleaning solutions on clothing or skin.

4. Ensure all piping connections are tight to avoid chemical leakage.

5. Ensure adequate ventilation.

6. Carefully follow manufacturer’s safety instructions on labels of

chemical containers and material safety data sheets.

7. Depressurize system prior to removing the cartridge pack.

8. Refer servicing to qualified personnel.

9. A full cartridge pack may weigh about 20 lbs.

Nanopure TOC - Analytical 2-1Thermo Scientific

Section 2 Introduction

Congratulations on your purchase of a Thermo Scientific Barnstead

Nanopure TOC - Analytical ultrapure water system. This water

purification system is designed to provide low TOC, high resistivity,

reagent grade water that exceeds ASTM Type I, ISO 3696 and CLSI-

CLRW Type I standards. It uses a four-stage deionization process

combined with a 0.2 micron filter to polish suitable feed water (distilled,

deionized, or reverse osmosis) to produce low TOC (<10 ppb) water with a

resistivity of up to 18.2 megohmcm. Water resistivity is continuously

monitored by a resistivity cell and displayed on a digital display. Actual

system TOC values, obtained by an integrated TOC analyzer, can be

concurrently displayed with the resistivity.

The electronics can be verified and calibrated utilizing a N.I.S.T. Traceable

Calibration module. See accessory ordering information.

Read the instructions carefully to ensure that you receive maximum benefit

from the Nanopure TOC - Analytical. Also, fill out and return the

enclosed warranty registration card as it will help us assure you of proper

warranty coverage.

General Usage

Do not use this product for anything other than its intended usage.

This manual suits for next models

Table of contents

Other Thermo Scientific Laboratory Equipment manuals

Thermo Scientific

Thermo Scientific Sorvall RC6 Plus User manual

Thermo Scientific

Thermo Scientific Savant Speedvac ISS110 User manual

Thermo Scientific

Thermo Scientific Heracell Vios 160i CR User manual

Thermo Scientific

Thermo Scientific Invitrogen Qubit Flex Fluorometer User manual

Thermo Scientific

Thermo Scientific FB1300 User manual

Thermo Scientific

Thermo Scientific MEGA-PURE 11A Water Still 677 Series User manual

Thermo Scientific

Thermo Scientific A 40B User manual

Thermo Scientific

Thermo Scientific Heraeus Megafuge 8 User manual

Thermo Scientific

Thermo Scientific TELESHAKE 1536-6 User manual

Thermo Scientific

Thermo Scientific RVT100 User manual

Thermo Scientific

Thermo Scientific TRACE 1300 User manual

Thermo Scientific

Thermo Scientific MaxQ 2000 User manual

Thermo Scientific

Thermo Scientific STANDARD Series User manual

Thermo Scientific

Thermo Scientific A2-OK Operating instructions

Thermo Scientific

Thermo Scientific Locator Series User manual

Thermo Scientific

Thermo Scientific Fisher Scientific Fisherbrand GT1R... User manual

Thermo Scientific

Thermo Scientific FH15 User manual

Thermo Scientific

Thermo Scientific Heratherm IMC 18 User manual

Thermo Scientific

Thermo Scientific Finnpipette FOCUS User manual

Thermo Scientific

Thermo Scientific Evolution Pro User manual

Thermo Scientific

Thermo Scientific mySPIN 6 User manual

Thermo Scientific

Thermo Scientific Dionex IonPac AS32-Fast-4mm Analytical User manual

Thermo Scientific

Thermo Scientific Finnpipette F1 User manual

Thermo Scientific

Thermo Scientific M79700 User manual

Popular Laboratory Equipment manuals by other brands

Qiagen

Qiagen DML 3000 user manual

Queensgate

Queensgate NANOSCAN OP400 Quick start instructions

Conviron

Conviron GEN1000-GE Operator's manual

Parr Instrument

Parr Instrument 4560 Operating instructions manual

IKA

IKA IC control operating instructions

Integra

Integra DOSE IT operating instructions

Agilent Technologies

Agilent Technologies 5800 ICP-OES user guide

Endress+Hauser

Endress+Hauser Cleanfit CPA875 operating instructions

NI PXI-5422 CALIBRATION PROCEDURE

Collomix

Collomix Aqix operating instructions

SPEX SamplePrep

SPEX SamplePrep 6875 Freezer/Mill Series operating manual

Ocean Insight

Ocean Insight FLAME-NIR+ Installation and operation manual

Parker

Parker ALIGN-MG-NA Installation, operation and maintenance manual

BD 644787 user guide

DENTAURUM

DENTAURUM Compact Megaplus Instructions for use

Biuged Laboratory Instruments

Biuged Laboratory Instruments BGD 626 instruction manual

VWR

VWR SAS Super IAQ instruction manual

illumina

illumina MiSeqDx reference guide