Bruker NMR CryoFIT User manual

CryoFIT

CryoProbe Flow Conversion System

Installation Manual

Version 003

Innovation with Integrity

●

NMR

system, or transmitted, in any form, or by any means without the prior consent of the

publisher. Product names used are trademarks or registered trademarks of their re-

spective holders.

This manual was written by

T. Marquardsen, J. Ganz

P/N: H12214

For further technical assistance for this product, please do not hesitate to contact your

nearest BRUKER dealer or contact us directly at:

Bruker Corporation

Am Silberstreifen

76287 Rheinstetten

Germany

Phone: + 49 721 5161 6155

E-mail: [email protected]

Internet: www.bruker.com

Contents

H12214_1_003 3

Contents

1 About This Manual .............................................................................................................................5

1.1 Policy Statement .................................................................................................................5

1.2 Symbols and Conventions ..................................................................................................5

2 Introduction.........................................................................................................................................7

3 Transport, Packaging and Storage ...................................................................................................9

3.1 Symbols on the Packaging .................................................................................................9

3.2 Inspection at Delivery........................................................................................................10

3.3 Packaging .........................................................................................................................11

3.4 Storage .............................................................................................................................11

4 Flow Hardware ..................................................................................................................................13

4.1 CryoFIT Accessory (PZ H13485)......................................................................................14

5 Installation.........................................................................................................................................15

5.1 Installation with a Warm CryoProbe..................................................................................15

5.2 Installation with a Cold CryoProbe....................................................................................16

5.3 Assembling the CryoFIT Accessory..................................................................................16

6 Inserting the Flow Cell .....................................................................................................................19

7 Removing the Flow Cell ...................................................................................................................29

8 Dismantling and Disposal................................................................................................................33

8.1 Dismantling .......................................................................................................................33

8.2 Disposal ............................................................................................................................33

9 Contact ..............................................................................................................................................35

List of Figures...................................................................................................................................37

Contents

4 H12214_1_003

About This Manual

H12214_1_003 5

1 About This Manual

This manual enables safe and efficient handling of the device.

This manual is an integral part of the device, and must be kept in close proximity to the

device where it is permanently accessible to personnel. In addition, instructions concerning

labor protection laws, operator regulations tools and supplies must be available and adhered

to.

Before starting any work, personnel must read the manual thoroughly and understand

its contents. Compliance with all specified safety and operating instructions, as well as local

work safety regulations, are vital to ensure safe operation.

The figures shown in this manual are designed to be general and informative and may not

represent the specific Bruker model, component or software/firmware version you are

working with. Options and accessories may or may not be illustrated in each figure.

1.1 Policy Statement

It is the policy of Bruker to improve products as new techniques and components become

available. Bruker reserves the right to change specifications at any time.

Every effort has been made to avoid errors in text and figure presentation in this publication.

In order to produce useful and appropriate documentation, we welcome your comments on

this publication. Support engineers are advised to regularly check with Bruker for updated

information.

Bruker is committed to providing customers with inventive, high quality products and services

that are environmentally sound.

1.2 Symbols and Conventions

Safety instructions in this manual are marked with symbols. The safety instructions are

introduced using indicative words which express the extent of the hazard.

In order to avoid accidents, personal injury or damage to property, always observe safety

instructions and proceed with care.

DANGER

DANGER indicates a hazardous situation which, if not avoided, will result in

death or serious injury.

This is the consequence of not following the warning.

1. This is the safety condition.

uThis is the safety instruction.

About This Manual

6 H12214_1_003

WARNING

WARNING indicates a hazardous situation, which, if not avoided, could result

in death or serious injury.

This is the consequence of not following the warning.

1. This is the safety condition.

uThis is the safety instruction.

CAUTION

CAUTION indicates a hazardous situation, which, if not avoided, may result in

minor or moderate injury or severe material or property damage.

This is the consequence of not following the warning.

1. This is the safety condition.

uThis is the safety instruction.

NOTICE

NOTICE indicates a property damage message.

This is the consequence of not following the notice.

1. This is a safety condition.

uThis is a safety instruction.

SAFETY INSTRUCTIONS

SAFETY INSTRUCTIONS are used for control flow and shutdowns in the event

of an error or emergency.

This is the consequence of not following the safety instructions.

1. This is a safety condition.

uThis is a safety instruction.

This symbol highlights useful tips and recommendations as well as

information designed to ensure efficient and smooth operation.

Introduction

H12214_1_003 7

2 Introduction

This document describes the installation of the CryoFITTM accessory, including the insertion

and removal of the flow cell.

Important Information

NOTICE

Risk of Material Damage Due to Improper Usage

Failure to observe the following safety warnings may result in material damage.

uNever try to spin the flow cell.

uNever use the sample lift if the flow cell is installed.

uDo not try to insert NMR sample tubes.

uDo not use the sample changer.

uDo not use the device with a BCU05 (freezing).

uMake sure the sample changer is not used during the flow application.

Introduction

8 H12214_1_003

Transport, Packaging and Storage

H12214_1_003 9

3 Transport, Packaging and

Storage

Retrofitting, repairs, adjustments or dismantling of the device must only be carried out by

Bruker Service or personnel authorized by Bruker. Damage due to servicing that is not

authorized by Bruker is not covered by your warranty.

3.1 Symbols on the Packaging

The following symbols are affixed to the packaging material. Always observe the symbols

during transport and handling.

Top The arrow tips on the sign mark the top of the

package. They must always point upwards;

otherwise the content may be damaged.

Fragile Marks packages with fragile or sensitive

contents.

Handle the package with care; do not allow the

package to fall and do not allow it to be

impacted.

Protect Against Moisture Protect packages against moisture and keep

dry.

Attach Here Lifting gear (lifting chain, lifting strap) must

only be attached to points bearing this symbol.

Center of Gravity Marks the center of gravity of packages.

Note the location of the center of gravity when

lifting and transporting.

Weight, Attached Load Indicates the weight of packages.

Handle the marked package in accordance

with its weight.

Permitted Stacking Load Indicates packages which are partially

stackable.

Do not exceed the maximum load-bearing

capacity specified on the symbol in order to

avoid damaging or destroying the content.

Transport, Packaging and Storage

10 H12214_1_003

Do not Damage Air-tight

Packaging

The packaging is air-tight. Damage to the

barrier layer may render the contents

unusable.

Do not pierce.

Do not use sharp objects to open.

Component Sensitive to

Electrostatic Discharge

The packaging contains components which

are sensitive to an electrostatic discharge.

Only allow packaging to be opened by trained

personnel.

Establish potential equalization before

opening.

Protect from Heat Protect packages against heat and direct

sunlight.

Protect from Heat and

Radioactive Sources

Protect packages against heat, direct sunlight

and radioactive sources.

Table3.1: Symbols on the Packaging

3.2 Inspection at Delivery

Upon receipt, immediately inspect the delivery for completeness and transport damage.

Proceed as follows in the event of externally apparent transport damage:

• Do not accept the delivery, or only accept it subject to reservation.

• Note the extent of the damage on the transport documentation or the shipper's delivery

note.

• Initiate complaint procedures.

Note:

Issue a complaint in respect to each defect immediately following detection. Damage

compensation claims can only be asserted within the applicable complaint deadlines.

Table of contents

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