Agilent Technologies 4100 Operating instructions

Agilent 4100

Microwave Plasma

Atomic Emission

Spectrometer

Site Preparation Guide

2 Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide

Notices

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Guide Part Number

G8000-90001

Edition

First edition, August 2011

Printed in USA

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Software is delivered and licensed as

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Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed

or adhered to, could result in

personal injury or death. Do not

proceed beyond a WARNING notice

until the indicated conditions are

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WARNING

CAUTION

Contents

Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide 3

Contents

1. Introduction 7

Installation Guidelines 8

Site Preparation Check-list 9

2. Safety Practices and Hazards 11

General 11

Plasma 12

Heat,VaporsandFumes 13

Compressed Gas Hazards 14

ElectricalHazards 15

OtherPrecautions 15

WarningSymbols 16

ColorCoding 17

CECompliance 18

ICES/NMB-001 18

3. Laboratory Environment 19

Suitability 19

Environmental Conditions 20

Temperaturecontrol 21

Cleanliness 21

Instrument cooling air supply 21

Workbench 22

Contents

4 Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide

WorkbenchLocation 22

PCRequirements 23

4. Instrument Shipping Information 25

In-houseTransitRoutes 25

InsuranceAfterDelivery 26

WeightsandDimensions 26

TransitDamage 27

Unpacking the Instrument 28

5. Laboratory Facilities 29

ExhaustSystem 29

ElectricalPowerSupplies 30

Electricalrequirements 31

Instrument power connections 31

Other electrical connections 32

Fuses 32

GasSupplies 32

Cylinder storage instructions 34

Cryogenicliquids 34

WasteFluidContainer 35

Guidelines for Software Installation 35

Contents

Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide 5

6. AccessoriesandOptions 37

Organic Solvents or Hydrofluoric Acid 37

ExternalGasControlModule 38

Gasrequirements 38

Monochromator Optics Air Purge 39

Gasrequirements 40

Sample Preparation System (SPS 3) 40

Environmental conditions 41

Multimode Sample Introduction System (MSIS) 41

Agilent 4107 Nitrogen Generator 42

Environmental requirements 42

Maximum sound power level 42

Gasrequirements 43

Electricalrequirements 44

Weights and dimensions 44

7. Gas Requirements and Configurations 45

Compressed Air Requirements 45

Agilent 4100 MP-AES Gas Configurations 48

Introduction

6 Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide

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Introduction

Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide 7

1. Introduction

Installation Guidelines 8

Site Preparation Check-list 9

This guide contains the information required to successfully prepare

a site for an Agilent 4100 Microwave Plasma Atomic Emission

Spectrometer (MP-AES) instrument installation.

On completion of the site preparation, fill in the check-list on Page 9,

(striking out those entries not applicable), and send this check-list to

your local Agilent agent or Agilent sales and service office. As soon

as it is received, Agilent or its agent will contact you to arrange a

convenient time for installation.

References to the Agilent 4100 MP-AES instrument are applicable to

all models and configurations unless otherwise stated.

In case of difficulty in preparing for the installation, and for details

of operator training courses, please contact your Agilent sales

representative or field service engineer at the address given below:

Introduction

8 Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide

Installation Guidelines

Allow a minimum of four hours for the installation by an Agilent field

service engineer. If accessories are included, allow a maximum of

eight hours.

The installation and familiarization will include the following

Instrument installation

Instrument software installation and registration

Accessory installation

Instrument installation performance tests

Basic customer training

Maintenance overview

Introduction

Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide 9

Site Preparation Check-list

I have prepared:

Exhaust system

Gas supplies

Nitrogen (separate supplies for the MP-AES and EGCM)

Air (separate supplies for the MP-AES and nitrogen

generator)

Argon

Electrical power supplies

Power connections

Personal computer with Windows 7 64-bit operating system

installed and printer

Waste container

Cooling air system (if required)

Accessories

SPS 3 – Sample Preparation System

EGCM – External Gas Control Module – including gas supplies

Monochromator Optics Purge – including gas supplies

Agilent 4107 Nitrogen Generator – including gas supplies

All preparations have been completed. Please arrange for the

installation to be completed as soon as possible. I understand that if

the installation site is not prepared in accordance with the enclosed

instructions, additional installation charges may be applicable.

Company name and address: 



Name:

Position:

Telephone: Date:

Preferred Installation date:

Signed:

Introduction

10 Agilent 4100 Microwave Plasma Atomic Emission Spectrometer Site Preparation Guide

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