Argonaut Technologies QUEST 210 User manual
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Instra
UAL
Part
Number
900114
ARGONAUT
TECHNOLOGIES
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
Quest 210 Manual Synthesizer
-
User Manual
Part Number 900
114
Revision 1.O,
5
September 2000
Copyright 02000by Argonaut Technologies
All rights reserved.
Argonaut Technologies
887 Industrial
Rd.,
Suite
G
San Carlos, CA 94070
Printed in the United States.
The information in this document has been carefully checked and is
believed to be entirely reliable. However, no responsibility is
assumed for inaccuracies. Statements in this document are not
intended to create any warranty, expressed or implied. Argonaut
reserves theright to make changes in any products herein to improve
reliability, function, or design. Argonaut does not assume any
liability arising out of the application oruse of any product
described herein; neither does it convey any license under its patent
rights nor the rights of others. Inclusion in this document does not
imply that any particular feature is standard on the instrument. The
information in this document is subject to change at any time.
Quest and pFrit are registered trademarks of Argonaut
Technologies, Inc. Teflon is a registered trademark of DuPont.
Tygon is a registered trademark of Norton Performance Plastics.
Other product names in this document are registered trademarks or
trademarks of their respective holders.
Revision
1.0
Quest
210
-
User
Manual
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
Limited Warranty
All individual instrument parts, consumables and the like are subject
to the provisions of the Seller Limited One
(1)
Year Warranty as
outlined below. Resin consumable products or the like are only
warranted to conform to the quantity and content stated on the label
at the time of delivery. All instrument system products are provided
subject to the provisions of the SELLER Limited One
(1)
Year
Warranty,
a
copy of which is available to Buyer and which is
incorporated herein in its entirety by this reference.
SELLER'S LIMITED ONE
(1)
YEAR WARRANTY IS
EXCLUSIVE AND IN LIEU OFALL OTHER WARRANTIES,
AND SELLER MAKES NO OTHER WARRANTIES, EXPRESS
OR IMPLIED, EITHER IN FACT OR BY OPERATION OFLAW,
STATUTORY OR OTHERWISE, AND SELLEREXPRESSLY
EXCLUDES AND DISCLAIMS ANY WARRANTY OF
MERCHANTABILITY OR FITNESS FOR A PARTICULAR
PURPOSE.
Limitation of Liability
Buyer agrees that SELLER's liability to Buyer in any way
connected with the sale andlor license of products or services to
Buyer, regardless of the form of action, shall in no event exceed the
price paid by Buyer for such products or services. Under no
circumstances will SELLER be liable for any damages resulting
from SELLER's failure to meet any delivery schedule, even if
SELLER has been advised of the possibility of such damages. IN
NO EVENT WILL SELLER BE LIABLE FOR COSTS OF
PROCUREMENT OFSUBSTITUTEPRODUCTS OR SERVICES,
LOST PROFITS, OR ANY SPECIAL INDIRECT,
CONSEQUENTIAL OR INCIDENTAL DAMAGES, HOWEVER
CAUSED AND ON ANY THEORY OFLIABILITY, ARISING IN
Quest
210
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UserManual Revision
1.0
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Exclusions
ANY WAY OUT OFTHE SALE AND/OR LICENSE OF
PRODUCTS OR SERVICES TO BUYER. THIS LIMITATION
SHALL APPLY EVEN
IF
SELLER HAS BEEN ADVISED OF
THEPOSSIBILITY OF SUCH DAMAGES AND
NOTWITHSTANDING ANY FAILURE OFESSENTIAL
PURPOSE OFANY LIMITED REMEDY.
This limited warranty covers normal use. Exclusions from this
limited warranty may include:
Servicing or modification by anyone other than a qualified
Argonaut Technologies Service Representative;
Non-conformance to recommended instrument operating
procedures as noted throughout this manual;
Failure to perform routine preventative maintenance;
Any natural disaster, including earthquake, lightning, tornado,
flood, or fire; electrical surges or the use of improper power
sources.
Revision
1.0
Quest
210
-
User
Manual
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
Warranty
Argonaut Warranty Agreement
Limited Warranty
Limitation of Liability
Exclusions
Contents
List
of
Figures
1
Introduction
Interference Information
Immunity Information
Quest
2
10Overview
Automated Solvent Wash Option
Gaseous Reaction and Concentration Manifold Option
2
Safety
User Attention Words
Warning Labels
Safety Class
System Safety
Safety Equipment
Operating Environment
Material Safety Data Sheets (MSDS)
3
System Overview
Reactor
Reaction Vessels
Luer Ports
Heating and Cooling
Reaction Mixing
Quest
210
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User
Manual
Revision
1.0
iii
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Agitator Magnets
Solvent/Gas Delivery System
Upper and Lower Manifolds
Manifold Control Valves
Low Pressure Gas Valve
Bubbler Port
Solvent Bottle Assembly
Product Collection
AutoWash Port
Waste Tray and Waste Reservoir
Controller
LCD Screen
Display Screens
Keypad
MODE Button
FORWARD and BACK Buttons
VALUE SETTING Buttons
HEAT ONIOFFButton
AGITATOR Control Buttons
Mix
Speed Valve
Controller Gas and Power Connections
Gas
Electrical Outlet
Power Switch
4
Quest
210
Installation
SitePreparation
Installation Requirements
Space
Gas
Electrical
Refrigeration
Materials
Components
Installation Glossary
Installation Procedure
Interface Harness Connections
SolventBottle Cap Assembly
Reactor Manifold Tubes
Waste Reservoir
Revision 1.0 Quest 210
-
UserManual
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Manifold Control Valves
Gas Connection
Single Gas Source
Dual Gas Source
Bubbler
Power Connection
SolventBottle
ASW
Option Installation
Overview
Installation Requirements
Space
Electrical Supply
Gas Supply
Waste Facilities
Ventilation
Installation Procedure
Location
Gas Connections
Power Connection
Controller and Reactor
ASW Module
SolventBottles
Installation Verification
Configuration
Manual Functions
Delivery Times
Automated Functions
6
Preparation For Synthesis
General
Line Power
Removing Reaction Vessels
Installing Reaction Vessels
Waste Reservoir
SolventBottle
Gas
7
Operation
Filling the Dead Volume
Quest
210
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User
Manual Revision
1.0
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Revision
1.0
Reagent and Solvent Delivery
Upper Manifold Membrane Valve
Parallel Delivery
Individual Delivery
Programming
Agitator Bar
Adjusting
Values
Starting and Stopping
Mix Speed
Temperature Control
Heating
Cooling
Draining Reaction Vessels
Non-Metered Draining
Metered Draining
Product Collection
8
Usingthe
ASW
Option
Programming
Program Number
Solvent Volume
Reactor Side
Draining Method
Variables
Wash Times
Washing
Monitoring The Wash
Editing Active values
Completion
Solvent Sparging
9
Cleaning
&
Maintenance
10
Tutorial
Overview
Summary of the Procedure
Preparation
Equipment Requirements
Reagent Requirements
Quest
210
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UserManual
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Reagent Preparation
Reductive Amination
Adding Reagent
Adding Sodium Borohydride
Product Work-Up and Collection
On-line Solid Phase Extraction
Off-Line Solid Phase Extraction
Cleaning and Maintenance
Manual Cleaning
Cleaning with the Automated Solvent Wash Module
Product Analysis
Tabulated Results and Structures
Spectroscopic Data
A
Glossary
B
Controller Screens
Start-upScreen
Firmware Version Screen
Menus
Agitator Values
Set Temperature
TemperatureMonitor Screen
Other Functions Menu
Set Contrast Menu
Self-Test Screen
Restore Defaults Screen
StartBtop Heaters Screen
C
Specifications
Quest 210
Automated Solvent Wash Option
D
Parts
&
Accessories
Quest
2
10Synthesizer
E
Service
Contact Information
Index
Quest
210
-
User
Manual
Revision
1.0
vii
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Other manuals for QUEST 210
1
Table of contents
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